Journal of Analytical Methods in Chemistry / 2020 / Article / Tab 4

Research Article

Establishment of a UPLC-MS/MS Method for Studying the Effect of Salt-Processing on Tissue Distribution of Twelve Major Bioactive Components of Qing’e Pills in Rats

Table 4

The extract recoveries and matrix effect of 12 compounds in rat kidney (n = 6).

CompoundConcentrations (ng/mL)Extract recovery (%)RSD (%)Matrix effect (%)RSD (%)

Psoralen587.98 ± 6.417.2894.20 ± 4.044.29
50087.93 ± 4.885.5693.42 ± 8.779.39
80085.67 ± 5.135.9990.85 ± 5.015.51

Isopsoralen588.74 ± 2.733.0893.86 ± 5.756.12
50088.60 ± 2.993.3891.92 ± 2.662.90
80088.99 ± 1.581.7892.27 ± 2.953.19

Psoralenoside12.5089.79 ± 4.104.5692.47 ± 2.242.42
100089.19 ± 0.941.0694.75 ± 0.560.59
160085.34 ± 1.601.8794.75 ± 0.710.75

Bavachin2.5087.75 ± 3.233.6993.05 ± 2.062.22
25088.84 ± 1.471.6693.96 ± 3.263.47
40089.48 ± 0.961.0793.99 ± 1.151.22

Isobavachin0.2588.02 ± 1.932.1993.64 ± 3.133.34
12585.59 ± 3.123.6495.01 ± 3.743.93
20088.69 ± 3.704.1796.38 ± 2.983.09

Bavachalcone1.2589.55 ± 1.411.5894.90 ± 0.600.64
5088.41 ± 1.301.4691.19 ± 2.132.34
8089.15 ± 1.081.2191.98 ± 1.051.14

Isobavachalcone2.5088.16 ± 0.911.0392.54 ± 1.101.19
25089.37 ± 0.981.1094.42 ± 1.041.10
40089.85 ± 0.760.8594.79 ± 0.780.82

Pinoresinol diglucoside2.5084.65 ± 4.014.7494.00 ± 3.433.65
5088.75 ± 1.091.2394.73 ± 1.001.06
8088.27 ± 1.421.6193.94 ± 1.451.55

Geniposidic acid2.5088.32 ± 2.993.3993.39 ± 2.752.94
100089.17 ± 0.710.7994.66 ± 1.531.62
160090.84 ± 0.971.0698.15 ± 1.891.93

Psoralidin2.5088.35 ± 2.612.9594.17 ± 1.912.03
50088.98 ± 1.011.1494.74 ± 1.241.31
80087.13 ± 3.363.8595.96 ± 0.350.36

Psoralen2.5088.45 ± 2.733.0993.34 ± 2.252.41
50081.59 ± 4.605.6388.22 ± 7.308.27
80085.60 ± 4.274.9994.39 ± 1.091.16

Isopsoralen2.5089.51 ± 2.682.9991.45 ± 2.943.22
25087.68 ± 3.153.5994.97 ± 3.763.96
40085.32 ± 6.027.0593.64 ± 1.861.99

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