Table of Contents
Journal of Catalysts
Volume 2015 (2015), Article ID 805714, 14 pages
Research Article

H-ZSM-5 Zeolite Synthesis by Sourcing Silica from the Wheat Husk Ash: Characterization and Application as a Versatile Heterogeneous Catalyst in Organic Transformations including Some Multicomponent Reactions

1Department of Chemistry, Shri Jagdishprasad Jhabarmal Tibrewala University (JJTU), Vidyanagari, Chudela, Jhunjhunu District, Rajasthan 333 001, India
2Post Graduate and Research Centre, Department of Chemistry, Poona College of Arts, Science and Commerce, Military Camp Area, Pune, Maharashtra 411 001, India
3Razak Institution of Skills, Education and Research (RISER), H.Q.: 1-9-722, Shrinagar, Near Rafaiya Masjid and Hanuman Mandir, Nanded, Maharashtra 431 605, India
4Division of Heterogeneous Catalysis, CSIR-National Chemical Laboratory (NCL), Dr. Homi Bhabha Road, Pune, Maharashtra 411 008, India
5Department of Chemistry, Dr. Harisingh Gour Central University (DHSGCU), Sagar, Madhya Pradesh, India
6School of Chemical Sciences, Swami Ramanand Teerth Marathwada University (SRTMU), Vishnupuri, Nanded, Maharashtra 431 601, India
7School of Earth Sciences, Swami Ramanand Teerth Marathwada University (SRTMU), Vishnupuri, Nanded, Maharashtra 431 601, India
8Department of Chemistry, Central University of Rajasthan (CURAJ), NH-8, Bandar Sindri, Kishangarh, Ajmer District, Rajasthan 305 801, India

Received 9 July 2014; Accepted 13 October 2014

Academic Editor: Sankaranarayana Pillai Shylesh

Copyright © 2015 Isak Rajjak Shaikh et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Supplementary Material

General Remarks: The chemicals procured from reputed suppliers were used in the present study and were either of analytic reagent (AR) or laboratory reagent (LR) grades. (TLC) using 0.25 mm silica gel plates monitored progress of each reaction in the present investigation by using silica gel as stationary phase and various combinations of solvents as mobile phase. Purity of the compounds was also checked by TLC. The melting points (MP) of purified organic product compounds were measured by taking solid compounds in capillary tubes using SUPERFIT India’s melting point measuring equipment and the MP values are uncorrected. Known compounds were first checked by comparing their melting point values to those of the available in literature. Apart from that IR and NMR techniques were employed for the spectral characterization of products synthesized. 1H NMR spectra were recorded at Varian’s Avance 400 MHz. The Infra Red (IR) spectra of the synthesized compounds were recorded on a Fourier Transform-Infra Red Spectrophotometer (Model Shimadzu 8700) using KBr pellets and values of Vmax are reported in cm−1.

  1. Supplementary Material