Journal of Chemistry

Journal of Chemistry / 2012 / Article

Open Access

Volume 9 |Article ID 514386 | https://doi.org/10.1155/2012/514386

Yan-Hua Cai, Shun-Jiang Li, "Synthesis and Performance of N-(Benzoyl) Stearic Acid Hydrazide", Journal of Chemistry, vol. 9, Article ID 514386, 8 pages, 2012. https://doi.org/10.1155/2012/514386

Synthesis and Performance of N-(Benzoyl) Stearic Acid Hydrazide

Received21 Mar 2011
Revised18 Aug 2011
Accepted04 Sep 2011

Abstract

N-(benzoyl) stearic acid hydrazide was synthesized from benzoyl hydrazine and stearyl chloride which was deprived from stearic acid via acylation. The structure of the compound had been characterized by FT-IR, 1H NMR, at the same time, the structure of N-(benzoyl) stearic acid hydrazide was optimized by the semiempirical method PM3. The influence of the reaction ratio, reaction time and reaction temperature to the yield of N-(benzoyl) stearic acid hydrazide was investigated by orthogonal experiment, and the optimized reaction condition was molar ratio of benzoyl hydrazine: stearyl chloride 1:1, reaction time 6 h, reaction temperature 70°C, and the yield was 92.9%. The TGA thermal analysis of N-(benzoyl) stearic acid hydrazide showed that thermal stability of N-(benzoyl) stearic acid hydrazide was affected by heating rate, and the N-(benzoyl) stearic acid hydrazide enhanced the tensile strength, modulus and elongation at break of Poly(L-lactic acid)(PLLA).

Copyright © 2012 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


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