Research Article

A Spectrophotometric Flow Injection Method for Determination of Ultratrace Amounts of Phenylhydrazine by Its Inhibition Effect on the Reaction of Thionin and Nitrite

Table 2

Determination of phenylhydrazine in real samples.

Sampl e a Concentration of phenylhydrazine added (μmol L−1)Concentration of phenylhydrazine found (μmol L−1)Recovery %

0.000
0.100 0 . 1 0 8 ± 0 . 0 0 2 108.00
Human serum0.200 0 . 1 8 5 ± 0 . 0 0 3 92.50
0.400 0 . 3 7 8 ± 0 . 0 0 1 94.50
0.500 0 . 5 2 7 ± 0 . 0 0 4 105.40

0.000
0.100 0 . 1 0 5 ± 0 . 0 0 5 105.00
River water (Zayandeh Rood)0.200 0 . 1 9 3 ± 0 . 0 0 2 96.50
0.400 0 . 3 8 9 ± 0 . 0 0 5 97.25
0.500 0 . 5 2 1 ± 0 . 0 0 7 104.20

a A verage from five determinations.