Research Article

Acetylation of Phenols, Anilines, and Thiols Using Silica Sulfuric Acid under Solvent-Free Conditions

Table 1

Solvent effect on acetylation of 4-chloroaniline by SSA at room temperature.

EntrySolventTime (min)Conversion (%)

1n-Hexane798
2CH3CN1098
3CH2Cl2798
4CHCl3590
5MeOH3085
6Neat398