Research Article

Synthesis and Characterization of Novel Thieno-Fused Bicyclic Compounds through New Enaminone Containing Thieno[2,3-b]pyridine Scaffold

Table 1


Crystal data
C15H15NO2S = 79.233 (1)°
= 273.35 = 2635.84 (16)
Triclinic, P-1 = 8
= 10.3859 (3) Mo radiation
= 13.8790 (6) = 0.24 mm−1
= 18.8006 (6) = 100 K
= 86.920 (1)°0.59 × 0.23 × 0.20 mm
= 82.081 (1)°

Data collection
Bruker APEX-II D8 venture diffractometer = 0.069
66528 measured reflections = 30.0°
15378 independent reflectionsStandard reflections: 0
9027 reflections with

Refinement
0 restraints
H atoms treated by a mixture of independent and constrained refinement
= 1.09 = 1.45 e 
15378 reflections = −0.43 e 
713 parameters