Research Article
Synthesis and Characterization of Novel Thieno-Fused Bicyclic Compounds through New Enaminone Containing Thieno[2,3-b]pyridine Scaffold
| Crystal data | C15H15NO2S | = 79.233 (1)° | = 273.35 | = 2635.84 (16) | Triclinic, P-1 | = 8 | = 10.3859 (3) | Mo Kα radiation | = 13.8790 (6) | = 0.24 mm−1 | = 18.8006 (6) | = 100 K | = 86.920 (1)° | 0.59 × 0.23 × 0.20 mm | = 82.081 (1)° | |
| Data collection | Bruker APEX-II D8 venture diffractometer | = 0.069 | 66528 measured reflections | = 30.0° | 15378 independent reflections | Standard reflections: 0 | 9027 reflections with | |
| Refinement | | 0 restraints | | H atoms treated by a mixture of independent and constrained refinement | = 1.09 | = 1.45 e | 15378 reflections | = −0.43 e | 713 parameters | |
|
|