Journal of Chemistry / 2017 / Article / Tab 1

Research Article

Synthesis, Characterization, and Catalytic Studies of Mn(III)-Schiff Base-Dicyanamide Complexes: Checking the Rhombicity Effect in Peroxidase Studies

Table 1

Crystal data and structure refinement for H2L2 and complex 1.

H2L2Complex 1

Chemical formulaC20H24N2O4C24H20MnN5O5
Formula weight356.41513.39
Crystal systemTriclinicTriclinic
Space group
Temperature (K)100100(2)
Volume (Å3)917.00(11)1093.74(11)
Radiation typeMo Mo
Crystal size (mm)0.2 × 0.11 × 0.030.12 × 0.11 × 0.06
, 0.942, 0.9970.9619, 0.9858
Number of measured reflections1193320087
Number independent reflections36074293
Reflections observed 20553209
Number of parameters247332
, (e Å−3)0.31, −0.280.338, −0.423

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