Optimization of the Extraction of the Volatile Fraction from Honey Samples by SPME-GC-MS, Experimental Design, and Multivariate Target Functions

Table 4

Results obtained for repeatability for the experiments of the experimental design: % of peaks in the chromatogram with CV% smaller than 5%, 10%, 20%, and 30%. Results in bold represent the maxima recorded for each threshold level.

	% CV < 5%	% CV < 10%	% CV < 20%	% CV < 30%
Exp 1	16	45	73	86
Exp 2	21	42	63	76
Exp 3	3.4	12	39	66
Exp 4	2.1	20	51	72
Exp 5	2.1	14	46	72
Exp 6	16	45	66	79
Exp 7	43	66	77	84
Exp 8	5.5	29	76	87
Exp 9	2.7	18	51	83