Green Synthesis Characterization and Thermotropic Behaviour of O-Linked Glycopyranosides of Phenolic Esters

Table 10

DSC transition temperatures of O-glycopyranosides.

Product code	1^st melting point, (°C)	2^nd melting point, (°C)	Crystallization point, TCr (°C)	Glass transition temperature, Tg (°C)
5a	75	134	28, 117, 219, 283	—
5b	67	133	31, 225	100
5c	71	146	17, 250	106
5d	87	287	183, 221, 254	—
5e	63	125	112, 212	96
5f	125	275	33, 250, 334, 434	—
5g	95	102	33, 390	217
5h	85	167	145, 320, 375	—
5i	130	325	25, 265, 385	115
5j	87	150	30, 265,410	130
5k	65	110	25, 220, 360	—
5l	75	166	35, 275	110