Research Article
Synthesis and Characterisation of Activated Carbon Obtained from Marula (Sclerocarya birrea) Nutshell
Table 5
Physicochemical characterisation of the synthesised high carbon samples.
| Temperature (°C) | Acid (%) | Physicochemical properties | pH | Moisture (%) | Ash (%) | Bulk density (g/cm3) | Iodine value (mg/g) |
| H2SO4treatments: | 200 | 20 | 2.9 ± 0.1a | 2.4 ± 0.2a | 0.65 ± 0.01a | 0.62 ± 0.02c | 1036.1 ± 0.01c | 40 | 3.9 ± 0.1b | 1.3 ± 0.1a | 3.49 ± 0.01b | 0.53 ± 0.01a | 938.5 ± 0.11a | 60 | 2.4 ± 0.1a | 10.7 ± 0.2c | 0.97 ± 0.01a | 0.54 ± 0.02a | 947.4 ± 0.12a | 400 | 40 | 6.1 ± 0.1c | 3.9 ± 0.1b | 51.0 ± 0.01c | 0.43 ± 0.01a | 1024.3 ± 0.10c | 20 | 5.7 ± 0.1c | 2.8 ± 0.2a | 3.79 ± 0.01b | 0.42 ± 0.01a | 1036.1 ± 0.12c | 40 | 5.7 ± 0.1c | 3.3 ± 0.1 | 4.62 ± 0.2b | 0.43 ± 0.02a | 915.2 ± 0.01a | 500 | 60 | 6.1 ± 0.1c | 2.5 ± 0.2a | 4.53 ± 0.01b | 0.45 ± 0.01a | 990.8 ± 0.15a | value | | <0.05 | <0.05 | <0.05 | <0.05 | <0.05 |
| H3PO4treatments: | 200 | 60 | 2.8 ± 0.1a | 6.4 ± 0.2a | 14.2 ± 0.01a | 0.54 ± 0.01a | 1042.6 ± 0.10a | 400 | 20 | 3.2 ± 0.1b | 6.6 ± 0.1a | 14.2 ± 0.01a | 0.42 ± 0.02a | 1048.3 ± 0.14a | 500 | 40 | 2.7 ± 0.1a | 14.6 ± 0.1b | 29.8 ± 0.01b | 0.82 ± 0.01b | 1075.7 ± 0.11a | 600 | 20 | 3.2 ± 0.b | 4.7 ± 0.2a | 11.3 ± 0.01a | 0.39 ± 0.02a | 1131.9 ± 0.13b | value | | <0.05 | <0.05 | <0.05 | <0.05 | <0.05 |
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Mean ± standard deviations are reported. Means in a column with different superscripts ( a, b, c) are significantly different at . |