Multiclass Pesticide Residue Analysis in Fruit and Vegetable Samples by Combining Acetone-Based Salting-Out Assisted Extraction with Dispersive Liquid-Liquid Microextraction

Table 5

Comparison of the proposed method with the other methods.

Methods	Analytes	LOD (µg/kg)	%RSD	Extraction time (min)	Extraction solvent volume (µL)	References
SPME-GC-MS	Bifenthrin	3	14	30	200	[36]
MAE-d-SPE-GC-MS	Carbofuran	6	10.9	9	15,000	[37]
Acetonitrile-based DLLME-GC-MS	Atrazine	6.2	2.2–9.0	NA^a	10,100	[20]
	Bifenthrin	2.6
	Chlorpyrifos	150
Acetone-based DLLME-HPLC-DAD	Carbofuran	4.7	4.2–9.5	3	5070	This work
	Atrazine	2.1
	Bifenthrin	2.3
	Chlorpyrifos	4.3

^aNot available.