Synthesis and Structural Study of Tris(𝝁-pyrazolyl)hexakis(pyrazole)dicobalt(III) Nitrate

Table 1

Crystal and experimental data.

Empirical formula	C42H61Co2N23O12
Formula weight	1198.00
Temperature (K)	150(1) K
Wavelength (Å)	0.71073 Å
Crystal system	Monoclinic
Space group	P21/m
Unit cell dimensions
	12.5977(3)
	15.3387(4)
	14.0800(3)
(°)	93.0868(15)
Volume (Å^3)	2716.76(11)
	2
(g cm^−3)	1.351
(MoKα) (mm^−1)	0.691
(000)	1248
range (°)	2.2–27.5
Limiting indices	−16 ≤ ≤ 16
	−19 ≤ ≤ 18
	−18 ≤ ≤ 18
Reflections collected/unique	11053/6431
Completeness (%)	99.5%
Goodness of fit on	1.036
indices [I > 2σ(I)]	= 0.0512, = 0.1305
indices (all data)	= 0.0755, = 0.1455
(Δρ)max, min	0.664, −0.522
(int)	0.0303