Synthesis and Structural Study of the Bis(ethylenediamine)CdFe(CO)₄ Monomer

Table 1

Crystal and experimental data.

Empirical formula	C8H16CdFeN4O4
Formula weight	400.50
Temperature (K)	150(1) K
Wavelength (Å)	0.71073 Å
Crystal system	Monoclinic
Space group	P21/a
Unit cell dimensions
a	14.4137(3)
b	7.6574(1)
c	14.5465(2)
β (°)	119.497(1)
Volume (Å^3)	1397.41(4)
Z	4
𝐷calcd (g cm^−3)	1.904
𝜇(MoK𝛼) (mm^−1)	2.571
F(000)	792
θ range (°)	1.61–27.48
Limiting indices	−18≤ℎ≤18
	−9≤𝑘≤9
	−18≤ℓ≤18
Reflections collected/unique	5999/3178
Completeness (%)	99.4%
Goodness of fit on 𝐹^2	1.093
𝑅 indices [𝐼>2𝜎(𝐼)]	𝑅1 = 0.0155, 𝑤𝑅2 = 0.0344
𝑅 indices (all data)	𝑅1 = 0.0186, 𝑤𝑅2 = 0.0355
(Δρ)max,min	0.375, −0.259
𝑅 (int)	0.0105