Synthesis, Characterization, and Crystal Structure of Pyridinium Tetrakis{1-trifluoromethyl-3-(1′-pyreno)-1,3-propanedionato}lanthanate(III) Complex

Table 1

Crystallographic data of the complex.

Empirical formula
Formula weight	1668.27
Temperature	90 K
Wavelength	0.71073 Å
Crystal system	Monoclinic
Space group	(No. 15)
Unit cell dimensions	Å	°
	Å
	Å
Volume	7365.3(8) Å^3
	4
Density (calculated)	1.504 g cm^−1
Absorption coefficient	0.673 mm^−1
(000)	3368
Crystal size	0.20 × 0.20 × 0.10 mm
Theta range for data collection	1.59 to 28.68°
Index ranges	, ,
	Reflections collected	42300
Independent reflections	8972
Reflections	8466 []
Completeness to theta = 28.68°	94.4%
Absorption correction	Empirical
Refinement method	Full-matrix least squares on
Data/restraints/parameters	8972/882/625
Goodness-of-fit on	1.075
Final indices []	,
indices (all data)	,
Largest diff. peak and hole (RMS deviation 0.157 e/Å^3)	3.656 and −2.052 eÅ^−3