Journal of Crystallography / 2014 / Article / Tab 1

Research Article

Synthesis and Molecular Structure of cis-Tetracarbonyl[N-(diphenylphosphino-kP)-naphthalen-1-yl-P,P-diphenylphosphinous amide-kP]chromium(0)

Table 1

Crystal data and structure refinement for 1.

FormulaC38H27CrNO4P2 4
675.55 [Mg m−3]1.342
Temp [K]150(2) (000)1392
Crystal systemMonoclinicAbs coeff [mm−1]4.053
Space groupP21/nNo. of rflns coll.24513
[Å]12.209(5)No. of indep rflns6488
[Å]20.003(5) 0.0223
[Å]13.954(5)No. of params415
α [°]90 1 0.0313
β [°]101.085(5)w 2 (all data)0.0869
γ [°]90 0.200
3]3344(2) −0.323