Table of Contents
Journal of Crystallography
Volume 2014, Article ID 704869, 6 pages
http://dx.doi.org/10.1155/2014/704869
Research Article

Crystallization and Structural Characterization of Dimeric and Trimeric Forms of (Neocuproine)CdFe(CO)4

Department of Chemistry, University of Utah, 315 South 1400 East, Room 2020, Salt Lake City, UT 84112-0850, USA

Received 24 October 2013; Accepted 22 January 2014; Published 11 March 2014

Academic Editor: Dong Qiu

Copyright © 2014 Torsten Kolb et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Linked References

  1. F. Feigl and P. Krumholz, “Über Salze des Eisencarbonylwasserstoffs,” Zeitschrift für Anorganische und Allgemeine Chemie, vol. 215, pp. 242–248, 1933. View at Google Scholar
  2. A. T. T. Hsieh, M. J. Mays, and R. H. Platt, “Infrared and Mössbauer spectra of tetracarbonylcadmioiron and related complexes,” Journal of the Chemical Society A, pp. 3296–3300, 1971. View at Publisher · View at Google Scholar · View at Scopus
  3. R. D. Ernst, T. J. Marks, and J. A. Ibers, “Metal-metal bond cleavage reactions. The crystallization and solid state structural characterization of cadmium tetracarbonyliron, CdFe(CO)4,” Journal of the American Chemical Society, vol. 99, no. 7, pp. 2090–2098, 1977. View at Google Scholar · View at Scopus
  4. H. Hock and H. Stuhlmann, “Über die Einwirkung von Quecksilbersalzen auf Eisenpentacarbonyl (II. Mitteil.),” Berichte der Deutschen Chemischen Gesellschaft, vol. 62, no. 2, pp. 431–437, 1929. View at Google Scholar
  5. R. D. Ernst and T. J. Marks, “Chemical and structural relationships among the oligomeric compounds MFe(CO)4 (M = Zn, Cd, Hg), PbFe(CO)4, AgCo(CO)4, and their base adducts,” Inorganic Chemistry, vol. 17, no. 6, pp. 1477–1484, 1978. View at Google Scholar · View at Scopus
  6. B. E. Zaugg, T. Kolb, A. M. Arif, and R. D. Ernst, “Structural studies of (pyridine)3ZnFe(CO)4 and (pyridine)(neocuproin)CdFe(CO)4,” Journal of Chemical Crystallography, vol. 40, no. 9, pp. 778–782, 2010. View at Publisher · View at Google Scholar · View at Scopus
  7. O. Fuhr and D. Fenske, “Syntheses and structure elucidations of novel (ironcarbonyl)zinc and -cadmium chloride derivatives,” Zeitschrift für Anorganische und Allgemeine Chemie, vol. 626, no. 8, pp. 1822–1830, 2000. View at Google Scholar · View at Scopus
  8. V. G. Albano, M. Monari, F. Demartin et al., “Synthesis and chemical behavior of [MFe4(CO)16]n- (M=Au, Zn, Cd, Hg) clusters: X ray structure of [NMe3CH2Ph]2[Au{ Fe2(CO)8}2]Cl and [PPh4]2[Cd{ Fe2(CO)6(μ-CO)2}2]2CH3CN,” Solid State Sciences, vol. 1, no. 7-8, pp. 597–606, 1999. View at Google Scholar · View at Scopus
  9. W. Deck, A. K. Powell, and H. Vahrenkamp, “Cluster mit Fe6Cd- und Fe6Hg-Baueinheiten,” Journal of Organometallic Chemistry, vol. 428, no. 3, pp. 353–362, 1992. View at Google Scholar · View at Scopus
  10. R. D. Ernst, T. J. Marks, and J. A. Ibers, “Metal-metal bond cleavage reactions. The crystal and molecular structure of (2,2′-bipyridyl)cadmium tetracarbonyliron, (bpy)CdFe(CO)4,” Journal of the American Chemical Society, vol. 99, no. 7, pp. 2098–2107, 1977. View at Google Scholar · View at Scopus
  11. R. J. Neustadt, T. H. Cymbaluk, R. D. Ernst, and F. W. Cagle Jr., “Crystallization and solid-state structural characterization of (2,2′-bipyridyl)zinc tetracarbonyliron, (bpy)ZnFe(CO)4,” Inorganic Chemistry, vol. 19, no. 8, pp. 2375–2381, 1980. View at Google Scholar · View at Scopus
  12. Z. Otwinowski and W. Minor, “Processing of X-ray diffraction data collected in oscillation mode,” Methods in Enzymology, vol. 276, pp. 307–326, 1997. View at Publisher · View at Google Scholar · View at Scopus
  13. A. Altomare, M. C. Burla, M. Camalli et al., “SIR97: a new tool for crystal structure determination and refinement,” Journal of Applied Crystallography, vol. 32, no. 1, pp. 115–119, 1999. View at Google Scholar · View at Scopus
  14. G. M. Sheldrick, “A short history of SHELX,” Acta Crystallographica A, vol. 64, no. 1, pp. 112–122, 2008. View at Publisher · View at Google Scholar · View at Scopus
  15. D. C. Creagh and W. J. McDauley, in International Tables for Crystallography: Mathematical, Physical and Chemical Tables, A. J. C. Wilson, Ed., chapter 4, pp. 206–222, Kluwer Academic Publishers, Dordrecht, The Netherlands, 1992.
  16. E. N. Maslen, A. G. Fox, and M. A. O'Keefe, in International Tables for Crystallography: Mathematical, Physical and Chemical Tables, A. J. C. Wilson, Ed., chapter 6, pp. 476–516, Kluwer Academic Publishers, Dordrecht, The Netherlands, 1992.
  17. L. J. Farrugia, “ORTEP-3 for windows—a version of ORTEP-III with a graphical user interface (GUI),” Journal of Applied Crystallography, vol. 30, no. 5, p. 565, 1997. View at Google Scholar · View at Scopus