Research Article

Solid State Structure of Bis[(bromo)(dicyclopentadienyl)vanadium(μ2-fluoro)][(bromo)(cyclopentadienyl)vanadium][tetrafluoroborate]

Table 1

Crystal and experimental data.

Empirical formulaC26H27BBr3Cl2F6V3

Formula weight927.74
Temperature (K)150(1)
Wavelength ()0.71073
Crystal systemMonoclinic
Space group
Unit cell dimensions
7.66490(10)
15.2457(2)
13.3185(2)
β (°)101.2721(8)
Volume ()1526.33(4)
2
(g cm−3)2.019
(MoKα) (mm−1)5.056
900
θ range (°)2.67–27.46
Limiting indices
Reflections collected/unique6956/3614
Completeness (%)99.9
Goodness of fit on 1.072
indices [],
indices (all data),
(int)0.0177
2.374, −2.321