Research Article
Functional and Oxidative Quality Characterization of Spray-Dried Omega-3-Enriched Milk Powder
Table 4
Analysis of variance (ANOVA) of the predicted second-order polynomial model for spray drying conditions’ impact on response parameters.
| Source of variation | df | Response parameters | EE (%) | EPA retained (g/100 g extracted fat) | DHA retained (g/100 g extracted fat) | PV (meqO2/kg) | Mean square | value | Mean square | value | Mean square | value | Mean square | value |
| Model | 14 | 8.74 | 0.0001 | 0.0155 | <0.0001 | 0.0609 NS | 0.2306 | 0.0148 | <0.0001 |
| Linear effects | A-IAT | 1 | 85.85 | <0.0001 | 0.1440 | <0.0001 | 0.2990 | 0.0167 | 0.1780 | <0.0001 | B-PS | 1 | 0.2763NS | 0.6183 | 0.0014 NS | 0.3566 | 0.0041 NS | 0.7582 | 0.0008 NS | 0.2253 | C-MD | 1 | 14.72 | 0.0021 | 0.0214 | 0.0022 | 0.1901 | 0.0485 | 0.0014 NS | 0.1124 | D-NS | 1 | 2.19 NS | 0.1724 | 0.0020 NS | 0.2765 | 0.0053 NS | 0.7239 | 0.0044 | 0.0099 |
| Interaction effects | AB | 1 | 0.0163 NS | 0.9034 | 0.0002 NS | 0.7105 | 0.0005 NS | 0.9132 | 0.0002 NS | 0.5126 | AC | 1 | 5.53 | 0.0379 | 0.0090 | 0.0301 | 0.0150 NS | 0.5552 | 0.0009 NS | 0.1997 | AD | 1 | 0.7966 NS | 0.4012 | 0.0009 NS | 0.4610 | 0.0018 NS | 0.8370 | 0.0000 NS | 0.8261 | BC | 1 | 1.37 NS | 0.2742 | 0.0064 NS | 0.0619 | 0.0086 NS | 0.6552 | 0.0004 NS | 0.3853 | BD | 1 | 2.71 NS | 0.1316 | 0.0042 NS | 0.1220 | 0.0095 NS | 0.6380 | 0.0000 NS | 0.8261 | CD | 1 | 0.3452 NS | 0.5780 | 0.0012 NS | 0.3913 | 0.0060 NS | 0.7080 | 0.0016 NS | 0.0939 |
| Quadratic effects | A² | 1 | 4.03 NS | 0.0711 | 0.0094 | 0.0272 | 0.0073 NS | 0.6804 | 0.0045 | 0.0088 | B² | 1 | 0.3485 NS | 0.5762 | 0.0001 NS | 0.8337 | 0.0424 NS | 0.3263 | 0.0000 NS | 0.8233 | C² | 1 | 0.1234 NS | 0.7385 | 0.0001 NS | 0.8501 | 0.3031 | 0.0161 | 0.0019 NS | 0.0725 | D² | 1 | 0.5206 NS | 0.4956 | 1.794E − 07NS | 0.9916 | 0.0493 NS | 0.2912 | 0.0004 NS | 0.3586 |
| Residual | 15 | 1.07 | — | 0.0016 | — | 0.0412 | — | 0.0005 | — | Lack of fit | 10 | 1.18 NS | 0.3677 | 0.0017 NS | 0.3923 | 0.0604 | 0.0018 | 0.0007 | 0.0132 | Pure error | 5 | 0.8352 | — | 0.0013 | — | 0.0029 | — | 0.0001 | — | Cor. total | 29 | — | — | — | — | — | — | — | — |
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,Significant at 0.05 level; IAT = inlet air temperature; PS = pump speed; MD = maltodextrin; NS = needle speed; EE = encapsulation efficiency; EPA = eicosapentaenoic acid; DHA = docosahexaenoic acid; PV = peroxide value. |