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Journal of Nanomaterials
Volume 2010, Article ID 671863, 5 pages
Research Article

One-Step Route to Synthesize Multiwalled Carbon Nanotubes Filled with MgO Nanorods

1Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education, Jinan 250100, China
2State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China
3Hefei National Laboratory for Physical Sciences at Microscale, Department of Chemistry, University of Science and Technology of China, Anhui, Hefei 230026, China

Received 2 November 2009; Accepted 19 April 2010

Academic Editor: Yanqiu Zhu

Copyright © 2010 Jing Liu et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


Multiwalled carbon nanotubes filled with MgO nanorods were synthesized through the reaction of ethanol and Mg powder in the presence of at 400 . X-ray powder diffraction indicated that the sample was composed of graphite and cubic MgO. Transmission electron microscopy studies showed that multi-walled CNTs with the outer diameters of 70–130 nm were filled with discontinuous MgO nanorods whose diameter was in the range of 25–40 nm. The ratios of the band intensities in Raman spectrum implied that carbon nanotubes had good crystallinity. The influence of correlative reaction factors on the morphology of the sample and the possible formation mechanism were discussed.