Microstructural Study of ZnO Nanostructures by Rietveld Analysis

Table 4

Crystallite domains and dimension ratio obtained by GIXRD and SEM (units in nanometers). *Poor quality in diffraction data.

Sample	GIXRD			SEM
	Crystallite domains, 𝐿hkl			L	D	L/D
	Normal to (002) planes	Normal to (100) planes	𝐿002/𝐿100
Z1	228	112	2.0	1341 ± 343	467 ± 109	2.9
Z2	264	119	2.2	1706 ± 317	422 ± 170	4.0
Z3	205	86	2.4	2221 ± 533	443 ± 123	5.0
Z4*	16*	73*	0.2*	1934 ± 375	369 ± 97	5.2
Z5	151	125	1.2	1283 ± 225	221 ± 58	5.8
Z6	136	118	1.2	1278 ± 233	238 ± 48	5.4
Z7	184	105	1.7	821 ± 175	115 ± 30	7.1
Z8	222	97	2.3	1280 ± 270	173 ± 45	7.4
Z9	140	92	1.5	1889 ± 329	444 ± 102	4.3
Z10	148	112	1.3	2109 ± 484	498 ± 73	4.2
Z11	154	126	1.2	1669 ± 377	599 ± 189	2.8
Z12	242	98	2.5	1762 ± 445	470 ± 126	3.7
Z13	295	91	3.2	1425 ± 420	331 ± 149	4.3
Z14	270	111	2.4	1803 ± 771	437 ± 182	4.1