Research Article
Formation of Mesoporous Materials from Silica Dissolved in Various NaOH Concentrations: Effect of pH and Ionic Strength
Table 2
Experimental conditions for the materials synthesized under various pH values and NaOH/SiO2 ratios and their pore characteristics.
| pH | Initial NaOH/SiO2 | Contained NaCl/SiO2 | Remained NaOH/SiO2 | Pore volume (cm3 g−1) | BET surface area (m2 g−1) |
| 10.8 | 0.5 | 0.08 | 0.42 | 0.66 | 863 | 10.7 | 0.5 | 0.16 | 0.34 | 0.51 | 673 | 10.5 | 0.5 | 0.24 | 0.26 | 0.76 | 915 | 10.4 | 0.5 | 0.26 | 0.24 | 0.73 | 840 | 10.2 | 0.5 | 0.32 | 0.18 | 0.56 | 718 |
| 11.1 | 1 | 0.32 | 0.68 | 0.22 | 437 | 10.7 | 1 | 0.48 | 0.52 | 0.58 | 949 | 10.5 | 1 | 0.56 | 0.44 | 0.73 | 975 | 10.4 | 1 | 0.64 | 0.36 | 0.67 | 845 | 10.2 | 1 | 0.72 | 0.28 | 0.66 | 780 |
| 11.1 | 2 | 1.2 | 0.8 | 0.24 | 394 | 11 | 2 | 1.28 | 0.72 | 0.15 | 254 | 10.7 | 2 | 1.36 | 0.64 | 0.6 | 892 | 10.6 | 2 | 1.44 | 0.56 | 0.76 | 992 | 10.5 | 2 | 1.48 | 0.52 | 0.65 | 837 | 10.3 | 2 | 1.6 | 0.4 | 0.59 | 748 |
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