Research Article
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
Table 1
Infrared peak positions and bond attributions in sample annealed at different temperatures and the comparison with the earlier literature reports.
|
Bonding | IR peak positions (cm−1) |
Respective references |
Values obtained for powder samples heated at |
Literature values and annealing temperature | 300°C | 350°C | 500°C | 600°C | 170°C | 400°C | 600°C |
| V–O–V bending | 488 | 488 | 497 | 495 | 450 | 476 | | [23, 24] | V–O–V stretching symmetric | 622 | 619 | 626 | 586 | 606 | 591 | 526 | [23–25] | V–O–V stretching asymmetric | 839 | 834 | 832 | 822 | 824 | 822 | 834 | [23–25] | V=O stretching symmetric | 1020 | 1020 | 1020 | 1020 | 1017 | 1018 | 1021 | [23–25] | C–H bending (scissoring) | 1384 | 1383 | 1383 | — | 1379 | | | [23] | C=O stretching | 1627 | 1650 | 1634 | — | 1633 | | | [23] |
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