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Journal of Nanomaterials
Volume 2016 (2016), Article ID 8393648, 10 pages
Research Article

Preparation of TiO2/Activated Carbon Composites for Photocatalytic Degradation of RhB under UV Light Irradiation

1School of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454003, China
2Department of Chemical Engineering, University of Newcastle, Callaghan, NSW 2308, Australia

Received 30 October 2015; Revised 23 December 2015; Accepted 26 January 2016

Academic Editor: Cunming Liu

Copyright © 2016 Baolin Xing et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


Photocatalysts comprising nanosized TiO2 particles on activated carbon (AC) were prepared by a sol-gel method. The TiO2/AC composites were characterized by X-ray diffraction (XRD), thermogravimetric (TG) analysis, nitrogen adsorption, scanning electron microscope (SEM), transmission electron microscope (TEM), and energy dispersive X-ray (EDX). Their photocatalytic activities were studied through the degradation of Rhodamine B (RhB) in photocatalytic reactor at room temperature under ultraviolet (UV) light irradiation and the effect of loading cycles of TiO2 on the structural properties and photocatalytic activity of TiO2/AC composites was also investigated. The results indicate that the anatase TiO2 particles with a crystal size of 10–20 nm can be deposited homogeneously on the AC surface under calcination at 500°C. The loading cycle plays an important role in controlling the loading amount of TiO2 and morphological structure and photocatalytic activity of TiO2/AC composites. The porosity parameters of these composite photocatalysts such as specific surface area and total pore volume decrease whereas the loading amount of TiO2 increases. The TiO2/AC composite synthesized at 2 loading cycles exhibits a high photocatalytic activity in terms of the loading amount of TiO2 and as high as 93.2% removal rate for RhB from the 400 mL solution at initial concentration of 2 × 10−5 mol/L under UV light irradiation.