Research Article
Response Surface Modelling of Electrosprayed Polyacrylonitrile Nanoparticle Size
Table 2
Uncoded variables for experimental and test data with corresponding responses.
| Number | Voltage (kV) | Concentration (% w/w) | Feed rate (mL/h) | Needle diameter (mm) | Mean particle size (nm) | Standard deviation (nm) |
| 1 | 10 | 1 | 0.263 | 1 | 190.24 | 29.76 | 2 | 10 | 1 | 0.263 | 0.8 | 172.61 | 26.11 | 3 | 10 | 1 | 0.263 | 0.6 | 157.89 | 24.43 | 4 | 10 | 1 | 0.789 | 1 | 205.59 | 28.42 | 5 | 10 | 1 | 0.789 | 0.8 | 201.63 | 30.32 | 6 | 10 | 1 | 0.789 | 0.6 | 180.62 | 30.74 | 7 | 10 | 1 | 1.315 | 1 | 216.66 | 31.94 | 8 | 10 | 1 | 1.315 | 0.8 | 198.08 | 30.05 | 9 | 10 | 1 | 1.315 | 0.6 | 185.75 | 31.77 | 10 | 10 | 2 | 0.263 | 1 | 200.2 | 31.54 | 11 | 10 | 2 | 0.263 | 0.8 | 184.26 | 28.14 | 12 | 10 | 2 | 0.263 | 0.6 | 179.89 | 29.64 | 13 | 10 | 2 | 0.789 | 1 | 227.99 | 36.64 | 14 | 10 | 2 | 0.789 | 0.8 | 208.58 | 29.58 | 15 | 10 | 2 | 0.789 | 0.6 | 196.21 | 28.06 | 16 | 10 | 2 | 1.315 | 1 | 223.26 | 34.2 | 17 | 10 | 2 | 1.315 | 0.8 | 207.55 | 31.7 | 18 | 10 | 2 | 1.315 | 0.6 | 198.68 | 30.89 | 19 | 10 | 3 | 0.263 | 1 | 153.72 | 19.26 | 20 | 10 | 3 | 0.263 | 0.8 | 150.7 | 18.11 | 21 | 10 | 3 | 0.263 | 0.6 | 142 | 24.25 | 22 | 10 | 3 | 0.789 | 1 | 192.73 | 22.66 | 23 | 10 | 3 | 0.789 | 0.8 | 175.5 | 25.41 | 24 | 10 | 3 | 0.789 | 0.6 | 155.67 | 22.55 | 25 | 10 | 3 | 1.315 | 1 | 183.05 | 24.18 | 26 | 10 | 3 | 1.315 | 0.8 | 169.37 | 28.68 | 27 | 10 | 3 | 1.315 | 0.6 | 162.08 | 23.35 | 28 | 12 | 1 | 0.263 | 1 | 170.66 | 25.24 | 29 | 12 | 1 | 0.263 | 0.8 | 165.22 | 30.33 | 30 | 12 | 1 | 0.263 | 0.6 | 138.01 | 24.96 | 31 | 12 | 1 | 0.789 | 1 | 202.16 | 28.4 | 32 | 12 | 1 | 0.789 | 0.8 | 185.58 | 36.26 | 33 | 12 | 1 | 0.789 | 0.6 | 178.41 | 30.04 | 34 | 12 | 1 | 1.315 | 1 | 207.8 | 27.76 | 35 | 12 | 1 | 1.315 | 0.8 | 192.2 | 34.24 | 36 | 12 | 1 | 1.315 | 0.6 | 184.85 | 31.73 | 37 | 12 | 2 | 0.263 | 1 | 171.72 | 26.39 | 38 | 12 | 2 | 0.263 | 0.8 | 160.35 | 25.68 | 39 | 12 | 2 | 0.263 | 0.6 | 156.23 | 22.78 | 40 | 12 | 2 | 0.789 | 1 | 205.23 | 27.74 | 41 | 12 | 2 | 0.789 | 0.8 | 190.16 | 27.68 | 42 | 12 | 2 | 0.789 | 0.6 | 183.81 | 22.4 | 43 | 12 | 2 | 1.315 | 1 | 222.27 | 33.65 | 44 | 12 | 2 | 1.315 | 0.8 | 211.59 | 29.07 | 45 | 12 | 2 | 1.315 | 0.6 | 193.61 | 31.75 | 46 | 12 | 3 | 0.263 | 1 | 144.05 | 15.35 | 47 | 12 | 3 | 0.263 | 0.8 | 129.18 | 16.5 | 48 | 12 | 3 | 0.263 | 0.6 | 122.88 | 20.33 | 49 | 12 | 3 | 0.789 | 1 | 163.97 | 20.19 | 50 | 12 | 3 | 0.789 | 0.8 | 148.94 | 19.96 | 51 | 12 | 3 | 0.789 | 0.6 | 155.36 | 21.66 | 52 | 12 | 3 | 1.315 | 1 | 179.37 | 20.45 | 53 | 12 | 3 | 1.315 | 0.8 | 166.75 | 25.52 | 54 | 12 | 3 | 1.315 | 0.6 | 163.76 | 19.41 | 55 | 14 | 1 | 0.263 | 1 | 162.35 | 20.76 | 56 | 14 | 1 | 0.263 | 0.8 | 149.83 | 20.7 | 57 | 14 | 1 | 0.263 | 0.6 | 140.41 | 23.51 | 58 | 14 | 1 | 0.789 | 1 | 191.61 | 27.24 | 59 | 14 | 1 | 0.789 | 0.8 | 177.17 | 26.99 | 60 | 14 | 1 | 0.789 | 0.6 | 169.67 | 31.52 | 61 | 14 | 1 | 1.315 | 1 | 195.59 | 33.24 | 62 | 14 | 1 | 1.315 | 0.8 | 189.03 | 30.25 | 63 | 14 | 1 | 1.315 | 0.6 | 184.73 | 29.45 | 64 | 14 | 2 | 0.263 | 1 | 182.99 | 24.71 | 65 | 14 | 2 | 0.263 | 0.8 | 153.93 | 25.04 | 66 | 14 | 2 | 0.263 | 0.6 | 156.55 | 25.65 | 67 | 14 | 2 | 0.789 | 1 | 212.26 | 26.03 | 68 | 14 | 2 | 0.789 | 0.8 | 185.32 | 29.13 | 69 | 14 | 2 | 0.789 | 0.6 | 172.25 | 24.09 | 70 | 14 | 2 | 1.315 | 1 | 207.86 | 30.44 | 71 | 14 | 2 | 1.315 | 0.8 | 194.31 | 32.21 | 72 | 14 | 2 | 1.315 | 0.6 | 180.52 | 24.11 | 73 | 14 | 3 | 0.263 | 1 | 146.34 | 18.94 | 74 | 14 | 3 | 0.263 | 0.8 | 129.74 | 20.75 | 75 | 14 | 3 | 0.263 | 0.6 | 112.78 | 19.34 | 76 | 14 | 3 | 0.789 | 1 | 179.25 | 21.56 | 77 | 14 | 3 | 0.789 | 0.8 | 145.38 | 21.84 | 78 | 14 | 3 | 0.789 | 0.6 | 142.37 | 23.51 | 79 | 14 | 3 | 1.315 | 1 | 188.52 | 25.61 | 80 | 14 | 3 | 1.315 | 0.8 | 172.44 | 27.9 | 81 | 14 | 3 | 1.315 | 0.6 | 159.78 | 29.9 |
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