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Journal of Nanotechnology
Volume 2012, Article ID 214783, 7 pages
Research Article

Fabrication of Bi-Doped TiO2 Spheres with Ultrasonic Spray Pyrolysis and Investigation of Their Visible-Light Photocatalytic Properties

1Department of Environmental and Life Sciences, Putian University, Putian 351100, China
2Nano and Advanced Materials Institute Limited, The Hong Kong University of Science and Technology, Hong Kong
3Department of Civil and Structural Engineering, Research Center for Environmental Technology and Management, The Hong Kong Polytechnic University, Hong Kong

Received 8 March 2012; Accepted 20 April 2012

Academic Editor: Reda M. Mohamed

Copyright © 2012 Jianhui Huang et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


Bismuth-doped TiO2 submicrospheres were synthesized by ultrasonic spray pyrolysis. The prepared bismuth-doped titania was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV-visible diffuse reflectance spectroscopy (UV-vis DRS), and X-ray photoelectron spectroscopy (XPS). Aqueous photocatalytic activity was evaluated by the decomposition of methyl orange under visible-light irradiation. The results indicate that doping of bismuth remarkably affects the phase composition, crystal structure, and the photocatalytic activity. The sample with 2% Bi exhibits the optimum photocatalytic activity.