Raman Spectroscopy, X-Ray, SEM, and DTA Analysis of
Alkali-Phosphate Glasses Containing <svg style="vertical-align:-4.47125pt;width:45.962502px;" id="M1" height="20.6" version="1.1" viewBox="0 0 45.962502 20.6" width="45.962502" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns="http://www.w3.org/2000/svg"><g transform="matrix(.022,-0,0,-.022,.062,14.975)"><path id="x57" d="M956 650v-28q-52 -7 -69 -22.5t-39 -77.5q-60 -175 -165 -533h-31l-175 499h-2l-163 -499h-31l-164 535q-18 60 -36 76.5t-65 21.5v28h243v-28q-53 -7 -63 -18.5t3 -49.5l122 -412h2l162 499h29l175 -500h2q87 277 113 401q12 45 0.5 59t-68.5 21v28h220z" /></g><g transform="matrix(.022,-0,0,-.022,20.999,14.975)"><path id="x4F" d="M381 665q131 0 226.5 -93t95.5 -239q0 -158 -96 -253t-238 -95q-137 0 -231 95t-94 238q0 142 92.5 244.5t244.5 102.5zM359 629q-89 0 -151 -74.5t-62 -208.5q0 -141 69 -233t175 -92q90 0 150.5 74t60.5 211q0 152 -69 237.5t-173 85.5z" /></g><g transform="matrix(.016,-0,0,-.016,37.738,20.35)"><path id="x33" d="M285 378v-2q65 -13 102 -54.5t37 -97.5q0 -57 -30.5 -104.5t-74 -75t-85.5 -42t-72 -14.5q-31 0 -59.5 11t-40.5 23q-19 18 -16 36q1 16 23 33q13 10 24 0q58 -51 124 -51q55 0 88 40t33 112q0 64 -39 96.5t-88 32.5q-29 0 -64 -11l-6 29q77 25 118 57.5t41 84.5
q0 45 -26.5 69.5t-68.5 24.5q-67 0 -120 -79l-20 20l43 63q51 56 127 56h1q66 0 107 -37t41 -95q0 -42 -31 -71q-22 -23 -68 -54z" /></g></svg> and Nb<sub>2</sub>O<sub>5</sub>

<table>SEM micrographs of the LiW-40 (a) and NaW-40 (b) samples heat-treated at 650°C for 4 hours.</table>

Journal of Spectroscopy

fig3

Figure 3

Figure 3: Raman Spectroscopy, X-Ray, SEM, and DTA Analysis of
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q0 45 -26.5 69.5t-68.5 24.5q-67 0 -120 -79l-20 20l43 63q51 56 127 56h1q66 0 107 -37t41 -95q0 -42 -31 -71q-22 -23 -68 -54z" /></g></svg> and Nb<sub>2</sub>O<sub>5</sub> 

Journal of Spectroscopy

Raman Spectroscopy, X-Ray, SEM, and DTA Analysis of Alkali-Phosphate Glasses Containing and Nb2O5

Figure 3

Raman Spectroscopy, X-Ray, SEM, and DTA Analysis of Alkali-Phosphate Glasses Containing and Nb₂O₅