Research Article

Analysis of 31 Hydrazones of Carbonyl Compounds by RRLC-UV and RRLC-MS(/MS): A Comparison of Methods

Table 1

Optimized mass spectrometry parameters for the detection of hydrazones.

ParameterOptimized value

Capillary (V)1,000
Skimmer (V) −33.1
Capillary outlet (V) −107.4
Octupole 1 DC (V) −4.4
Octupole 2 DC (V)−1.37
Trap drive (V) 40.03
Octupole RF (V) 136
Lens 1 (V)0.82
Lens 2 (V) 33.6
Trap drive30
Target 30,000