Research Article

Synthesis of Nanoscale T i O 2 and Study of the Effect of Their Crystal Structure on Single Cell Response

Figure 2

Differential curves of the pore size distribution in series 1 samples obtained by hydrolysis of TiCl4 under the following conditions: (a) samples 1.1–1.3, T = 4°C; (b) samples 1.4–1.6, T = 20°C; (c) samples 1.7–1.9, T = 70°C (pH: ○—3 ÷ 4, ■—6 ÷ 7, ∆—9 ÷ 10); and (d) series 3 samples obtained by hydrolysis of TIP ( 𝑇 s y n t h e s i s : ■—50°C, ∆—70°C, □—95°C). Pore size distribution was determined by BET.
498345.fig.002a
(a)
498345.fig.002b
(b)
498345.fig.002c
(c)
498345.fig.002d
(d)