Research Article

A Simple and Green Procedure for the Synthesis of 5-Arylidenerhodanines Catalyzed by Diammonium Hydrogen Phosphate in Water

Table 1

Effect of different reaction conditions on synthesis of 5-arylidenerhodaninesa.

Entry(NH4)2HPO4 (mol%)Temperature (°C)Time (min)Yield (%)b

110804585
210901886
3101001886
4090600
55901875
620901886

Reaction condition: 2,4-dichlorobenzaldehyde (2.5 mmol), rhodanine (2.5 mmol), and water (3 mL).
Isolated yield.