Journal of Crystallography

Research Article

Synthesis and Crystal Structure of trans-Diiodobis(piperidine-1-carbonitrile)platinum(II)

Table 1

Crystallographic details for trans-[PtI2(NCNC5H10)2].
Empirical formulaC12H20I2N4Pt
Fw669.21
Temp. (K)100(2)
( )0.71073
Cryst systMonoclinic
Space group 21/c
a ( )6.7497(7)
b ( )15.8212(16)
c ( )8.2773(8)
(deg)104.110(4)
( )857.25(15)
Z 2
(Mg/m3)2.593
(Mo K ) (mmāˆ’1)11.779
Number of reflections27391
Unique reflections4203
GOOF (F2)1.229
0.0257
R1a ( )0.0160
wR2b ( )0.0377
R1 = . wR2 = [ / ]1/2.