Journal of Crystallography

Research Article

Synthesis, Crystal Structure, and Characterization of a New Organic-Inorganic Hybrid Material:

Table 2

Selected bond distances (Å) and angles (°) for (H3AEP)2·(BiCl6)·3Cl·2H2O.
Selected bond length (Å)
Bi1–Cl12.781 (2)N1–C31.50 (1)
Bi1–Cl22.675 (2)C1–C21.49 (1)
Bi1–Cl32.705 (2)C3–C41.50 (1)
Bi1–Cl42.749 (2)N2–C21.52 (1)
Bi1–Cl52.719 (2)N2–C41.496 (8)
Bi1–Cl62.644 (2)N2–C51.50 (1)
N1–C11.49 (1)C5–C61.48 (1)
Selected angles (°)
Cl6–Bi1–Cl291.15 (7)Cl6–Bi1–Cl1176.60 (7)
Cl6–Bi1–Cl388.49 (7)Cl2–Bi1–Cl185.48 (7)
Cl2–Bi1–Cl387.00 (6)Cl3–Bi1–Cl190.84 (7)
Cl6–Bi1–Cl588.08 (7)Cl5–Bi1–Cl192.43 (7)
Cl2–Bi1–Cl590.39 (6)Cl4–Bi1–Cl187.56 (7)
Cl3–Bi1–Cl5175.65 (6)C3–N1–C1111.9 (7)
Cl6–Bi1–Cl495.77 (7)C5–N2–C4113.1 (5)
Cl2–Bi1–Cl4172.41 (7)C5–N2–C2110.0 (6)
Cl3–Bi1–Cl490.07 (6)C4–N2–C2108.3 (6)
Cl5–Bi1–Cl492.94 (6)C9–N4–C7112.3 (7)