Research Article
Synthesis and Crystal Structure of 1-Methyl-3-(2-pyridyl)imidazolium Hexafluorophosphate
Table 1
Crystal data and data collection parameters for the compound (MeIMPy)(PF6).
| Identification code | 1 | Empirical formula | C9H10N3F6P | Formula weight | 305.17 | Temperature | 100(2) K | Crystal system, space group | Monoclinic, 2(1)/ | Unit cell dimensions | (8) Å | (16) Å | (11) Å | (2)° | Volume | 1162.1(2) Å3 | , calculated density | 4, 1.744 mg/m3 | Absorption coefficient | 0.305 mm−1 | (000) | 616 | Crystal size | mm3 | range for data collection | 2.40 to 28.31° | Index ranges | , , | Reflections collected | 7402 | Independent reflections | 2885 [(int) = 0.0189] | Completeness to theta | 98.0% | Data/restraints/parameters | 2826/0/173 | Goodness-of-fit on F2 | 1.190 | Final indices | 1 = 0.0446a, 2 = 0.1119 | indices (all data) | 1 = 0.0592a, 2 = 0.1611b | Largest diff. peak and hole | 0.526 and −0.691 e·Å−3 |
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