Research Article
Synthesis and Molecular Structure of cis-Tetracarbonyl[N-(diphenylphosphino-kP)-naphthalen-1-yl-P,P-diphenylphosphinous amide-kP]chromium(0)
Table 1
Crystal data and structure refinement for 1.
| Formula | C38H27CrNO4P2 | | 4 | | 675.55 | [Mg m−3] | 1.342 | Temp [K] | 150(2) | (000) | 1392 | Crystal system | Monoclinic | Abs coeff [mm−1] | 4.053 | Space group | P21/n | No. of rflns coll. | 24513 | [Å] | 12.209(5) | No. of indep rflns | 6488 | [Å] | 20.003(5) | | 0.0223 | [Å] | 13.954(5) | No. of params | 415 | α [°] | 90 | 1 | 0.0313 | β [°] | 101.085(5) | w2 (all data) | 0.0869 | γ [°] | 90 | | 0.200 | [Å3] | 3344(2) | | −0.323 |
|
|