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Journal of Crystallography
Table of Contents
Journal of Crystallography
/
2014
/
Article
/
Tab 2
/
Research Article
Structural Studies of
and
Table 2
Selected bond lengths (Å) and angles (°) for [(py)
2
CdFe(CO)
4
]
3
.
Bond distances
Cd1–Fe1
2.6645(8)
Cd2–N3
2.441(4)
Cd1–Fe2
2.6833(7)
Cd2–N3A
2.429(10)
Fe1–C1
1.747(7)
C1–O1
1.158(7)
Fe1–C2
1.767(6)
C2–O2
1.151(7)
Fe1–C3
1.784(7)
C3–O3
1.156(7)
Fe1–C4
1.767(6)
C4–O4
1.164(7)
Fe2–C5
1.765(6)
C5–O5
1.162(7)
Fe2–C6
1.779(7)
C6–O6
1.163(7)
Cd1–N1
2.424(4)
Cd2–Fe1
2.6429(8)
Cd1–N2
2.444(5)
Bond angles
Fe1–Cd1–Fe2
135.31(3)
Fe1–Cd2–Fe1′
139.51(4)
Cd1–Fe1–Cd2
102.52(3)
Cd1–Fe2–Cd1′
104.62(4)
C1–Fe1–C2
93.2(3)
C5–Fe2–C5′
92.7(4)
C3–Fe1–C4
138.2(3)
C6–Fe2–C6′
135.8(4)
Cd1–Fe1–C2
79.8(2)
N1–Cd1–N2
87.39(16)
Cd2–Fe1–C1
84.7(2)
N3–Cd2–N3′
88.2(4)
Cd1–Fe2–C5′
81.6(2)
N3′–Cd2–N3A
86.7(2)