Research Article
Synthesis, Characterization, and X-Ray Crystal Structure of Bis(O-amyl dithiocarbonato-κ2S,S′)bis(4-cyanopyridine-κN)nickel(II)
Table 1
Crystallographic data for the title compound.
| CCDC number | 893165 | Empirical formula | C24H30N4O2S4Ni | Formula weight | 593.47 | Temperature (K) | 293(2) | Shape | Block shaped | Color | Dark green | Crystal system | Orthorhombic | Space group | P b c a | Unit cell dimensions (, °) | | | 11.455(5) | | 9.602(4) | | 26.374(1) | | 90.00 | | 90.00 | | 90.00 | Volume (), Z | 2900.8(2), 4 | Dimension (mm3) | | (gcm−3) | 1.359 | (mm−1) | 0.984 | (000) | 1240 | 2 range for data collection (°) | 3.56–26.00 | Limiting indices | | | | Reflection collected | 18668 | Independent reflection | 2850 | Goodness-of-fit on | 1.104 | Data/restraint/parameter | 2850/6/179 | Final indices | 0.0499 | indices (all data) | 0.0781 | Largest difference peak and hole (e nm−3) | 358 and −263 |
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