Research Article
Synthesis, Characterization, and X-Ray Crystal Structure of Bis(O-amyl dithiocarbonato-κ2S,S′)bis(4-cyanopyridine-κN)nickel(II)
Table 2
Selected bond distances (
) and bond angles (°).
| Bond distances | | | | Ni1–N10 | 2.121(3) | Ni1–S2 | 2.433(1) | Ni1–S1 | 2.441(9) | S1–C3 | 1.691(4) | S2–C3 | 1.691(4) | C3–O4 | 1.320(4) | O4–C5 | 1.453(5) | C5–C6 | 1.482(6) | N10–C11 | 1.338(4) | N10–C15 | 1.341(4) | Bond angles | | | | N10–Ni1–S2 | 91.10(8) | N10–Ni1–S1 | 90.29(8) | S2–Ni1–S1 | 105.70(3) | C3–S1–Ni1 | 82.22(1) | C3–S2–Ni1 | 82.47(1) | O4–C3–S2 | 122.9(3) | O4–C3–S1 | 116.1(3) | S2–C3–S1 | 121.0(2) | N17–C16–C13 | 177.6(5) | | |
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