Research Article
Synthesis, Crystal Structure, and Hirshfeld Surface Analysis of Ciprofloxacin-Salicylic Acid Molecular Salt
Table 1
The crystal and experimental data.
| | Empirical formula | C24H24FN3O7 | | Formula weight | 485.46 | | Crystal system | Triclinic | | Space group | P-1 | | (K) | 298(1) | | () | 0.71070 | | () | 6.9532(10) | | () | 9.8979(11) | | () | 17.212(2) | | (°) | 79.397(19) | | (°) | 85.53(2) | | (°) | 83.09(2) | | () | 1154.0(3) | | 2 | | (g cm−3) | 1.397 | | (mm−1) | 0.109 | | (0 0 0) | 508 | | Crystal size (mm) | | | Crystal shape and color | Prism, colorless | | (°) | 2.4 to 27.4 | | −8→7 | | −12→12 | | −21→21 | | Reflections collected | 4623 | | Reflections unique | | | Absorption correction | Multi-scan | | Goodness-of-fit on | 1.18 | | and indices (all data) | 0.055, 0.057 | | , (e·) | 0.26 and −0.29 | | CCDC | 968489 |
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