Research Article
Crystal Structure of a 9-Subunit Archaeal Exosome in Pre-Catalytic States of the Phosphorolytic Reaction
Table 1
Data collection and refinement statistics.
| Rrp4/Rrp41D182A/Rrp42 space group P213 | Pi | RNA * Pi |
| Data collection | | | Wavelength () | 0.98012 | 0.97995 | Unit cell (), | 135.1 | 134.8 | Resolution () | 40–1.8 (1.9–1.8) | 40–2.5 (2.65–2.50) | sym | 0.082 (0.653) | 0.125 (0.722) | I/ | 11.4 (1.6) | 14.5 (2.9) | Completeness | 0.973 (0.901) | 0.999 (1.00) | Redundancy | 5.0 (2.7) | 7.1 (7.1) |
| Refinement | | | Resolution () | 40–1.8 (1.9–1.8) | 40–2.5 (2.6–2.5) | No. of reflections | 71709 | 28497 | work | 0.183 (0.346) | 0.191 (0.325) | free | 0.221 (0.375) | 0.255 (0.376) | R.m.s deviations | | | Bond lengths (Å) | 0.017 | 0.009 | Bond angles (°) | 1.6 | 1.5 | PDB code | 4ba1 | 4ba2 |
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Highest-resolution shell is shown in parenthesis.
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