Table of Contents
Chromatography Research International
Volume 2011, Article ID 684369, 8 pages
http://dx.doi.org/10.4061/2011/684369
Research Article

Development and Validation of HPTLC Method for Estimation of Carbamazepine in Formulations and Its In Vitro Release Study

1A. R. College of Pharmacy and G. H. Patel Institute of Pharmacy, Sardar Patel University, Vallabh Vidyanagar 388 120, India
2Indukaka Ipcowala College of Pharmacy, Sardar Patel University, New Vallabh Vidyanagar 388 121, India

Received 31 July 2010; Accepted 18 September 2010

Academic Editor: Irene Panderi

Copyright © 2011 Rashmin B. Patel et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Linked References

  1. N. S. Barakat, S. A. Omar, and A. A. E. Ahmed, “Carbamazepine uptake into rat brain following intra-olfactory transport,” Journal of Pharmacy and Pharmacology, vol. 58, no. 1, pp. 63–72, 2006. View at Publisher · View at Google Scholar · View at Scopus
  2. T. K. Vyas, A. K. Babbar, R. K. Sharma, S. Singh, and A. Misra, “Intranasal mucoadhesive microemulsions of clonazepam: preliminary studies on brain targeting,” Journal of Pharmaceutical Sciences, vol. 95, no. 3, article 8, pp. 570–580, 2006. View at Publisher · View at Google Scholar · View at Scopus
  3. M. J. Lawrence and G. D. Rees, “Microemulsion-based media as novel drug delivery systems,” Advanced Drug Delivery Reviews, vol. 45, no. 1, pp. 89–121, 2000. View at Publisher · View at Google Scholar
  4. F. Jaffery, S. N. Ahmad, and B. L. Jailkhani, “A spectrophotometric method for simultaneous estimation of phenytoin and carbamazepine,” Journal of Pharmacological Methods, vol. 9, no. 1, pp. 33–39, 1983. View at Publisher · View at Google Scholar · View at Scopus
  5. L. E. Riad, K. K. H. Chan, W. E. Wagner Jr., and R. J. Sawchuk, “Simultaneous first- and zero-order absorption of carbamazepine tablets in humans,” Journal of Pharmaceutical Sciences, vol. 75, no. 9, pp. 897–900, 1986. View at Google Scholar · View at Scopus
  6. M. S. Cámara, C. Mastandrea, and H. C. Goicoechea, “Chemometrics-assisted simple UV-spectroscopic determination of carbamazepine in human serum and comparison with reference methods,” Journal of Biochemical and Biophysical Methods, vol. 64, no. 3, pp. 153–166, 2005. View at Publisher · View at Google Scholar · View at Scopus
  7. Z. Rezaei, B. Hemmateenejad, S. Khabnadideh, and M. Gorgin, “Simultaneous spectrophotometric determination of carbamazepine and phenytoin in serum by PLS regression and comparison with HPLC,” Talanta, vol. 65, no. 1, pp. 21–28, 2005. View at Publisher · View at Google Scholar · View at Scopus
  8. A. J. Fellenberg and A. C. Pollard, “A rapid spectrophotometric procedure for the simultaneous micro determination of carbamazepine and 5,5 diphenyl hydantoin in blood,” Clinica Chimica Acta, vol. 69, no. 3, pp. 429–431, 1976. View at Google Scholar · View at Scopus
  9. C. Huang, Q. He, and H. Chen, “Flow injection photochemical spectrofluorimetry for the determination of carbamazepine in pharmaceutical preparations,” Journal of Pharmaceutical and Biomedical Analysis, vol. 30, no. 1, pp. 59–65, 2002. View at Publisher · View at Google Scholar
  10. A. Frigerio, K. M. Baker, and G. Belvedere, “Gas chromatographie degradation of several drugs and their metabolites,” Analytical Chemistry, vol. 45, no. 11, pp. 1846–1851, 1973. View at Google Scholar
  11. K. Chen and H. K. Bashi, “Comparative analysis of antiepileptic drugs by gas chromatography using capillary or packed columns and by fluorescence polarization immunoassay,” Journal of Analytical Toxicology, vol. 15, no. 2, pp. 82–85, 1991. View at Google Scholar · View at Scopus
  12. M. E. Auer, U. J. Griesser, and J. Sawatzki, “Qualitative and quantitative study of polymorphic forms in drug formulations by near infrared FT-Raman spectroscopy,” Journal of Molecular Structure, vol. 661-662, no. 1–3, pp. 307–317, 2003. View at Publisher · View at Google Scholar · View at Scopus
  13. S. Mennickent, R. Fierro, M. Vega, M. de Diego, and C. G. Godoy, “Instrumental planar chromatographic method for determination of carbamazepine in human serum,” Journal of Separation Science, vol. 32, no. 9, pp. 1454–1458, 2009. View at Publisher · View at Google Scholar · View at Scopus
  14. T. D. Cyr, F. Matsui, R. W. Sears, N. M. Curran, and E. G. Lovering, “Liquid chromatographic methods for assay of carbamazepine, 10,11-dihydrocarbamazepine, and related compounds in carbamazepine drug substance and tablets,” Journal of the Association of Official Analytical Chemists, vol. 70, no. 5, pp. 836–840, 1987. View at Google Scholar · View at Scopus
  15. M. E. Abdel-Hamid, “Comparative LC-MS and HPLC analyses of selected antiepileptics and beta-blocking drugs,” Farmaco, vol. 55, no. 2, pp. 136–145, 2000. View at Publisher · View at Google Scholar · View at Scopus
  16. M. K.M. Babu, “Simultaneous separation and quantitation of four antiepileptic drugs—a study with potential for use in patient drug level monitoring,” Journal of Pharmaceutical and Biomedical Analysis, vol. 34, no. 2, pp. 315–324, 2004. View at Publisher · View at Google Scholar
  17. M. W. Lam, C. J. Young, R. A. Brain et al., “Aquatic persistence of eight pharmaceuticals in a microcosm study,” Environmental Toxicology and Chemistry, vol. 23, no. 6, pp. 1431–1440, 2004. View at Publisher · View at Google Scholar
  18. C. González-Barreiro, M. Lores, M. C. Casais, and R. Cela, “Simultaneous determination of neutral and acidic pharmaceuticals in wastewater by high-performance liquid chromatography-post-column photochemically induced fluorimetry,” Journal of Chromatography A, vol. 993, no. 1-2, pp. 29–37, 2003. View at Publisher · View at Google Scholar · View at Scopus
  19. R. B. Miller and M. Vranderick, “A validated HPLC method for the determination of carbamazepine and carbamazepine 10,11-epoxide in human plasma,” Journal of Liquid Chromatography, vol. 16, no. 6, pp. 1249–1261, 1993. View at Google Scholar · View at Scopus
  20. E. S. Walker, “Liquid chromatographic determination of carbamazepine in tablets,” Journal of the Association of Official Analytical Chemists, vol. 71, no. 3, pp. 523–525, 1988. View at Google Scholar
  21. N. S. Rajadhyaksha, S. P. Jain, and P. D. Amin, “Carbamazepine: stability indicating HPLC assay method,” Analytical Letters, vol. 40, no. 13, pp. 2506–2514, 2007. View at Publisher · View at Google Scholar · View at Scopus
  22. A. Owen, J. N. Tettey, P. Morgan, M. Pirmohamed, and B. K. Park, “LC determination of carbamazepine in murine brain,” Journal of Pharmaceutical and Biomedical Analysis, vol. 26, no. 4, pp. 573–577, 2001. View at Publisher · View at Google Scholar · View at Scopus
  23. F. Demirkaya and Y. Kadioǧlu, “Determination of carbamazepine using RP-HPLC method in pharmaceutical preparations,” FABAD Journal of Pharmaceutical Sciences, vol. 30, no. 2, pp. 78–82, 2005. View at Google Scholar · View at Scopus
  24. E. K. Oh, E. Ban, J. S. Woo, and C.-K. Kim, “Analysis of carbamazepine and its active metabolite, carbamazepine-10,11- epoxide, in human plasma using high-performance liquid chromatography,” Analytical and Bioanalytical Chemistry, vol. 386, no. 6, pp. 1931–1936, 2006. View at Publisher · View at Google Scholar · View at Scopus
  25. R. B. Patel, M. B. Shankar, M. R. Patel, and K. K. Bhatt, “Simultaneous estimation of acetylsalicylic acid and clopidogrel bisulfate in pure powder and tablet formulations by high-performance column liquid chromatography and high-performance thin-layer chromatography,” Journal of AOAC International, vol. 91, no. 4, pp. 750–755, 2008. View at Google Scholar · View at Scopus
  26. R. B. Patel, A. B. Patel, M. R. Patel, M. B. Shankar, and K. K. Bhatt, “Estimation of alprazolam and sertraline in pure powder and tablet formulations by high-performance liquid chromatography and high-performance thin-layer chromatography,” Analytical Letters, vol. 42, no. 11, pp. 1588–1602, 2009. View at Publisher · View at Google Scholar · View at Scopus
  27. M. R. Patel, R. B. Patel, J. R. Parikh, and B. G. Patel, “HPTLC method for estimation of tazarotene in topical gel formulations and in vitro study,” Analytical Methods, vol. 2, no. 3, pp. 275–281, 2010. View at Publisher · View at Google Scholar
  28. R. B. Patel, M. R. Patel, K. K. Bhatt, and B. G. Patel, “HPTLC method development and validation: quantification of paliperidone in formulations and in vitro release study,” Analytical Methods, vol. 2, no. 5, pp. 525–531, 2010. View at Publisher · View at Google Scholar
  29. R. B. Patel, M. R. Patel, K. K. Bhari, and B. G. Patel, “Development and validation of an HPTLC method for determination of olanzapine in formulations,” Journal of AOAC International, vol. 93, no. 3, pp. 811–819, 2010. View at Google Scholar
  30. ICH Guideline Q2(R1), “Validation of analytical procedures: text and methodology,” November 2005, http://www.ich.org/LOB/media/MEDIA417.pdf.
  31. R. B. Patel, M. R. Patel, M. B. Shankar, and K. K. Bhatt, “Development and validation of second-derivative spectrophotometry method for simultaneous estimation of Alprazolam and Fluoxetine hydrochloride in pure powder and tablet formulation and its comparison with HPLC method,” Eurasian Journal of Analytical Chemistry, vol. 4, no. 1, pp. 76–86, 2009. View at Google Scholar