Research Article

Development and Validation of RP-HPLC Method for Quantitative Estimation of Vinpocetine in Pure and Pharmaceutical Dosage Forms

Table 3

Accuracy studies of vinpocetine in standard and drug-matrix solutions.

Amount added (μgmL−1)Peak areaAmount recovered (μgmL−1)% RecoveryRecovery (Mean ±  %RSD)

Standard solution1602758830160.12100.08
1602757741160.06100.04100.05 ± 0.023
1602757692160.05100.04
1803108421180.41100.23
1803108988180.44100.25100.24 ± 0.012
1803109134180.45100.25
2003463527201.02100.51
2003463889201.04100.52100.52 ± 0.009
2003464117201.05100.53
2203811741221.23100.56
2203812077221.25100.57100.56 ± 0.007
2203811562221.22100.56
2404168397241.93100.80
2404167556241.88100.78100.79 ± 0.012
2404167502241.88100.78

Drug-matrix solution1602773303160.96100.60
1602772297160.90100.56100.57 ± 0.024
1602772063160.89100.56
1803119142181.03100.60
1803121001181.14100.66100.63 ± 0.030
1803119725181.06100.62
2003477174201.81100.90
2003477005201.80100.90100.91 ± 0.015
2003477987201.86100.92
2203831775222.39101.10
2203831000222.35101.08101.08 ± 0.025
2203829872222.28101.05
2404185580242.92101.20
2404186378242.97101.22101.21 ± 0.011
2404185596242.92101.20