Research Article

Practical Implication of Chromatographic Method for Estimation of Aceclofenac and Pregabalin in Bulk and Pharmaceutical Dosage Forms

Table 6

Summary of validation parameters.

ParameterAceclofenacPregabalin

Linearity
 Regression equation
 Regression coefficient ()0.9990.999
 Range (µg/mL)5–253.75–18.75
 Accuracy (% mean recovery) ()98.45–100.0899.69–100.48
Precision (% CV)
 Repeatability ()1.321.55
 Intraday precision ()0.91–1.290.72–1.07
 Interday precision ()1.32–1.980.94–1.77
 LOD (µg/mL)0.640.35
 LOQ (µg/mL)1.951.06
 SpecificityCompliedComplied
 RobustnessCompliedComplied