Validated Stability Indicating Chromatographic Method for the Simultaneous Estimation of Camylofin with NSAID Drugs and a New Approach of Method Transfer from Classical HPLC to a Modern UPLC Instrument

Table 3

Content uniformity study results.

Sets	Content uniformity study
	Method precision		Intermediate precision
	% assay		% assay
	CMF	DCF	CMF	DCF
Set 1	99.27	99.26	99.35	100.14
Set 2	99.03	98.51	100.18	99.81
Set 3	98.98	99.71	99.92	100.16
Set 4	98.99	98.89	98.88	99.11
Set 5	99.02	98.58	98.94	99.15
Set 6	98.58	100.07	99.84	99.79
Set 7	100.13	99.33	98.94	100.07
Set 8	99.44	100.02	98.87	99.99
Set 9	99.60	98.64	100.04	99.87
Set 10	100.21	99.77	99.19	98.79
Mean of % assay	99.33	99.28	99.42	99.69
% RSD	0.53	0.60	0.53	0.49
Mean of absolute % bias	0.328	1.306	0.419	1.722