Chromatography Research International / 2016 / Article / Tab 3

Research Article

Validated Stability Indicating Chromatographic Method for the Simultaneous Estimation of Camylofin with NSAID Drugs and a New Approach of Method Transfer from Classical HPLC to a Modern UPLC Instrument

Table 3

Content uniformity study results.

SetsContent uniformity study
Method precisionIntermediate precision
% assay% assay

Set 199.2799.2699.35100.14
Set 299.0398.51100.1899.81
Set 398.9899.7199.92100.16
Set 498.9998.8998.8899.11
Set 599.0298.5898.9499.15
Set 698.58100.0799.8499.79
Set 7100.1399.3398.94100.07
Set 899.44100.0298.8799.99
Set 999.6098.64100.0499.87
Set 10100.2199.7799.1998.79

Mean of % assay99.3399.2899.4299.69
% RSD0.530.600.530.49
Mean of absolute % bias0.3281.3060.4191.722

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