|
| Method | Detector | Column | Mobile phase | Flow rate (mL/min) | Detection wavelength | (min) | Recovery % | Linearity | LOD | LOQ |
|
| B P [19] | UV | ODS C18, (100 × 4.6 mm)
3 µm | MeOH : H2O
(50 : 50 v/v) | 0.8 | 224 nm | 8 | — | — | — | — |
| Ref [8] | UV | Hypersil (ODS 250 × 4.6 mm, 5 µm) | ACN : Buffer | 1.0 | 215 nm | 3.0371 | 100 | 20–120 µg/mL ( = 0.9980) | 0.644 µg/mL | 1.951 µg/mL |
| Ref [20] | UV | Hypersil ODS C18 (250 × 4.6 mm, 5 µm) | MeOH : Buffer
(60 : 40 v/v) | 1.0 | 270 nm | 2 | 100.12 | 60–140 µg/mL ( = 0.9990) | 10 µg/mL | 15 µg/mL |
| Ref [21] | DAD | Hypersil ODS C18 (100 × 4.0 mm, 3 µm) | ACN : Buffer (18 : 72 v/v) | 0.3 | 220 nm | 6 | 94–100.2 | 2–50 µg/mL ( = 0.9998) | — | 2 µg/mL |
| Ref [22] | UV | Phenomenex ODS2, C18, (250 × 4.6 mm, 5 µm) | TEA : ACN : MeOH (50 : 25 : 25 v/v) | 2.0 | 235 nm | 2.183 | 99 | 200–300 µg/mL ( = 0.9996) | 3.40 µg/mL | 10.31 µg/mL |
| Ref [23] | UV-Vis | Phenomenex C18 (150 × 4.6 mm, 5 µm) | MeOH : orthophosphoric acid (50 : 50 v/v) | 0.6 | 271 nm | 3.49 | 101.12 | 1–10 µg/mL ( = 0.9872) | 0.05 µg/mL | 0.5 µg/mL |
| Ref [24] | UV | ODS C18 (250 × 4.6 mm × 5 µm) | ACN : Buffer (50 : 50 v/v) | 1.0 | 226 nm | 2.9 | 94–112 | 80–120 µg/mL ( = 0.999) | 3.3 µg/mL | 10 µg/mL |
| Ref [25] | PDA | Inertsil ODS3 (250 × 4.6 mm, 5 µm) | ACN : Buffer (20 : 80 v/v) | 1.0 | 220 nm | 7.6 | 94–105 | 5–25 g/mL ( = 0.996) | 0.007 g/mL | 0.022 g/mL |
| Ref [26] | UV | Xterra (250 × 4.6 mm, 5 µm) | ACN : Buffer (gradient elution) | 1.5 | 265 nm | — | 100–102 | 0.00625–0.15 µg/mL ( = 0.9999) | 0.008 µg/mL | 0.075 µg/mL |
| Ref [27] | UV-Vis | Phenomenex Luna C18 (150 × 4.6 mm, 5 µm) | ACN : MeOH : buffer (20 : 50 : 30 v/v) | 1.0 | 250 nm | 3.34 | 100.2 | 1–10 µg/mL ( = 0.9997) | 0.164 µg/mL | 0.5 µg/mL |
| Ref [28] | PDA | Xterra ODS C18 (4.6 × 150 × 5 µm) | H2O : MeOH (50 : 50 v/v) | 0.8 | 230 nm | 2.442 | 100–102 | 50–150 µg/mL ( = 0.999) | 0.00003 µg | 0.0001 µg |
| Ref [29] | UV-Vis | Zorbax C18 (4.6 × 250 mm, 5 µm) | Buffer : ACN : TEA
(95 : 5 : 0.1 v/v) | 0.9 | 280 nm | 4.489 | 101.17 ± 1 | 1.25–25 µg/mL ( = 0.9992) | 1.012 µg/mL | 3.067 µg/mL |
| Ref [30] | UV-Vis | Phenomenex Gemini C18 (250 × 4.6 mm × 5 µm) | Buffer : MeOH : ACN (30 : 35 : 35 v/v) | 1.5 | 240 nm | 2.2 | 98.99 | 20–30 µg/mL ( = 0.9980) | 54.13 µg/mL | 164.03 µg/mL |
| Ref [31] | UV | Hypersil BDS, (250 × 4.6 mm, 5 µm) | ACN : TEA (40 : 60 v/v) | 1.0 | 228 nm | 3.3 | 100 ± 2 | 6.25–37.5 µg/mL ( = 0.9999) | 0.075 µg/mL | 0.224 µg/mL |
| Ref [32] | PDA | Phenomenex Gemini C18 (250 × 4.6 mm, 5 µm) | ACN : Buffer (70 : 30 v/v) | 1.0 | 254 nm | 4.25 | 98.65 | 2.5–12.5 µg/mL ( = 0.9995) | 5.0 ng/mL | 15 ng/mL |
| Ref [33] | PDA | Hypersil BDS C18 (250 × 4.6 mm, 5 µm) | MeOH/ACN
(70 : 30 v/v) | 1.0 | 254 nm | 3.4 | 100 | 20–80 µg/mL ( = 0.999) | 0.13 µg/mL | 0.05 µg/mL |
| Present study | PDA | Inertsil ODS3 C18, (4.6 × 250 mm, 5 µm) | ACN : H2O (50 : 50 v/v) | 1.0 | 272 nm | 3.5 | 99.93 | 2–30 µg/mL ( ≥ 0.9978) | 0.5 µg/mL | 1.7 µg/mL |
|
