Research Article
Synthesis and Structural Characterization of a New Tetranuclear Nickel(II) Sulfato Complex Containing the Anionic Form of Di-2-Pyridyl Ketone Oxime
Table 2
Selected interatomic distances (Å) and angles (°) for 1.
| | Ni1-O1 | 2.046 (3) | Ni2-O2 | 2.071 (3) | | Ni1-O2 | 2.046 (3) | Ni2-O3 | 2.042 (3) | | Ni1-O4 | 2.033 (3) | Ni2-O7 | 2.163 (3) | | Ni1-O8 | 2.048 (3) | Ni2-N1 | 2.090 (3) | | Ni1-N5 | 2.090 (3) | Ni2-N2 | 1.997 (4) | | Ni1-N6 | 2.074 (3) | Ni2-N4 | 2.053 (3) |
| | O1-Ni1-O2 | 89.59 (11) | O2-Ni2-O3 | 94.82 (11) | | O1-Ni1-O4 | 101.65 (11) | O2-Ni2-O7 | 88.69 (10) | | O1-Ni1-O8 | 173.53 (11) | O2-Ni2-N1 | 169.13 (12) | | O1-Ni1-N5 | 82.89 (11) | O2-Ni2-N2 | 90.44 (12) | | O1-Ni1-N6 | 83.38 (12) | O2-Ni2-N4 | 84.07 (12) | | O2-Ni1-O4 | 84.24 (11) | O3-Ni2-O7 | 176.29 (10) | | O2-Ni1-O8 | 88.62 (11) | O3-Ni2-N1 | 88.91 (12) | | O2-Ni1-N5 | 107.12 (11) | O3-Ni2-N2 | 95.11 (12) | | O2-Ni1-N6 | 170.67 (12) | O3-Ni2-N4 | 87.08 (12) | | O4-Ni1-O8 | 84.36 (12) | O7-Ni2-N1 | 87.86 (11) | | O4-Ni1-N5 | 167.92 (13) | O7-Ni2-N2 | 86.05 (12) | | O4-Ni1-N6 | 91.16 (12) | O7-Ni2-N4 | 92.09 (12) | | O8-Ni1-N5 | 91.70 (12) | N1-Ni2-N2 | 79.04 (13) | | O8-Ni1-N6 | 99.02 (12) | N1-Ni2-N4 | 106.36 (13) | | N5-Ni1-N6 | 78.16 (13) | N2-Ni2-N4 | 174.25 (13) |
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