International Journal of Inorganic Chemistry
Volume 2015, Article ID 121895, 11 pages
http://dx.doi.org/10.1155/2015/121895
Synthesis, Characterization, and Structural Assessment of Ni(II) Complexes Derived from Bis(2-hydroxy-1-naphthaldehyde)succinoyldihydrazone
1Department of Chemistry, University of Technology and Management, Shillong, Meghalaya 793003, India
2Department of Chemistry, Indian Institute of Technology Patna, Bihar 801103, India
3Department of Chemistry, North-Eastern Hill University, Shillong, Meghalaya 793022, India
Received 3 September 2015; Revised 2 November 2015; Accepted 3 November 2015
Academic Editor: Alfonso Castiñeiras
Copyright © 2015 Mithun Chakrabarty et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Supplementary Material
Fig.S1: Infrared spectrum of bis(2-hydroxy-1-naphthaldehyde)succinoyldihydrazone (H4nsh) in KBr.
Fig.S2: Infrared spectrum of [Ni(H2nsh)(py)2]. H2O (2) in KBr.
Fig.S3: Infrared spectrum of [Ni(H2nsh)(2-pic)2] (3) in KBr.
Fig.S4: Infrared spectrum of [Ni2(nsh)(H2O)4] (6) in KBr.
Fig.S5: Infrared spectrum of [Ni2(nsh)(py)4].4H2O (7) in KBr.
Fig.S6: Infrared spectrum of [Ni2(nsh)(4-pic)4].4H2O(10) in KBr.
Fig.7: TGA/DTA curve of complex [Ni(H2nsh)(H2O)2] (1).
Fig.8: TGA/DTA curve of complex [Ni2(H2nsh)(H2O)4].H2O (6).
Fig.9: TGA/DTA curve of complex [Ni2(nsh)(py)4].4H2O (7).
Fig.10: TGA/DTA curve of complex [Ni2(nsh)(2-pic)4].4H2O (8).