Research Article
Synthesis and Characterization of
Table 1
Summary of crystallographic data of [2-CH3CH2C6H4NH3]6P6O18·4H2O.
| Chemical formula | [2-CH3CH2C6H4NH3]6P6O18·4H2O | Molecular weight | 1279.00 | Temperature, K | 293 | Wavelength, Å | 0.71073 | Crystal system | monoclinic | Space group, | P21/c, 2 | , , , Å | 16.220(4), 10.220(5), 20.328(4) | , deg | 113.24(3) | , Å3 | 3096.5(18) | , g/cm3 | 1.372 | , mm−1 | 0.252 | (000) | 1352 | Crystal sizes, mm | | Crystal shape | Prism | range for data collection, deg | 3.21, 29.97 | Independent reflections | 8617 | Reflections/restraints/ parameters | 8404/63/315 | | 0.072 | | 0.157 | Goodness-of-fit | 0.995 | Maximum and minimum residual electron density, e/Å3 | 0.85 and −0.42 |
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