Table of Contents
ISRN Nanotechnology
Volume 2011, Article ID 582534, 7 pages
Research Article

Preparation of TiO2 Nanoparticle/Nanotube Composites via a Vapor Hydrolysis Method and Their Photocatalytic Activities

1State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, Donghua University, Shanghai 201620, China
2Engineering Research Center of Advanced Glasses Manufacturing Technology, MOE, Donghua University, Shanghai 201620, China

Received 23 June 2011; Accepted 15 August 2011

Academic Editors: A. Hu, A. N. Obraztsov, A. Swami, and N. Tabet

Copyright © 2011 Weiwei Yu et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


TiO2 nanoparticle/nanotube composites were prepared by a vapor hydrolysis method and were characterized by X-ray diffraction, transmission electron microscopy, and N2 isothermal adsorption-desorption. The well-crystallized TiO2 nanoparticles were uniformly deposited onto the surface of TiO2 nanotubes. The photocatalytic activity of the composites was evaluated by the degradation of acid red G and phenol solution under UV irradiation. The results showed that the photocatalytic activities of the modified composites were significantly enhanced compared to the pristine nanotubes. In particular, the 50 wt% TiO2 nanoparticle/nanotube composite obtained at 120°C exhibited a remarkable ARG degradation efficiency of 90% after irradiation for 30 minutes and a phenol degradation efficiency of 93% after irradiation for 2 hours.