Research Article
Determination of Picogram Levels of Roxithromycin in Pharmaceutical, Human Serum, and Urine by Flow-Injection Chemiluminescence
Table 4
Results of determination for ROX in spiked human urine.
| Sample no. | Added (pg mL−1) | Found (pg mL−1) | RSD (%) |
Recovery (%) |
ROX content (μg mL−1) Sample/spiked |
| 1 | 0 | 4.3 | 1.8 | 96.7 | 4.2/4.5 | 3.0 | 7.2 | 2.5 | 2 | 0 | 9.8 | 2.9 | 90.0 | 9.6/10.0 | 3.0 | 12.5 | 2.2 | 3 | 0 | 35.8 | 2.3 | 102.0 | 36.0/36.2 | 20.0 | 56.2 | 1.9 | 4 | 0 | 20.8 | 2.1 | 98.0 | 20.7/21.0 | 10.0 | 30.6 | 3.0 |
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