Research Article
In-Cell Clean-Up Pressurised Liquid Extraction Method to Determine Pesticides in Mushroom Compost by Gas Chromatography-Tandem Mass Spectrometry
Table 1
MS/MS parameters for the detection of analytes and internal standard.
| Compound | Time, min | Parent ion, m/z | Quantification ion, m/z | Isolation window, m/z | Ionization | ESLa | REVb |
| Diazinon | 15.3–16.5 | 305 | 169 + 249 | 5 | CI | 120.0 | 86.0 | Caffeine (IS) | 16.5–17.5 | 194 | 193 | 3 | EI | 74.7 | 60.0 | Iprodione | 17.5–23.5 | 314 | 245 + 271 | 3 | EI | 121.0 | 81.0 | Prochloraz | 23.5–25.5 | 308 | 244 + 175 | 3 | EI | 118.8 | 83.0 | Deltamethrin | 25.5–28.0 | 253 | 172 + 174 | 3 | EI | 97.5 | 64.0 |
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(a) Excitation storage level, m/z. (b) Resonant excitation amplitude, V.
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