Research Article

Use of Functionalized Resin for Matrix Separation and Trace Elements Determination in Petroleum Produced Formation Water by Inductively Coupled Plasma Mass Spectrometry

Table 1

Instrumental parameters used for the analytes determination by ICP-MS after solid-phase extraction.

ICP-MS operating parameters setting

Cool gas flow (L min−1)13
Auxiliary gas flow (L min−1)0.8
Nebulizer gas flow (L min−1)0.95
Plasma power (W)1400
Sample uptake rate (mL min−1)0.90
Resolution300
Analytes (measured isotopes)60Ni, 59Co, 65Cu, 111Cd and 208Pb
Internal standards45Sc, 72Ge, 103Rh, 115In
Dwell time (ms)10
Channels per AMU1
Data acquisition modeContinuous acquisition
Runs3
Spray chamberGlass impact bead
NebulizerMeinhard glass concentric